The serial number of a dispersion unit is found on its rear panel. Statistics shows the mean, standard deviation, maximum and minimum of a group of selected measurement records. Making Your Mobile Life Easier. The display will change. This is the purpose of the sample dispersion units. Equivalent maximum length this is where the diameter of a theoretical sphere is the same as the maximum dimension of the original particle. Mastersizer 2000 Page 5-3, 66 Chapter 5 Viewing the results Changing the Records tab By default the Records tab displays seven fields which include Record number, Sample name, Source, Measured on, etc. For clarity, this manual assumes that the primary dispersion unit for each system is as follows: For the Mastersizer 2000 the Hydro 2000G. Page 4-16 MAN 0384, 53 Making measurements - a tutorial Chapter 4 do any additives need to be added to the sample to aid dispersion (and what quantity)? Admixtures are added in larger quantities, typically 1g/ l. A list of commonly used admixtures is given below: Sodium Hexametaphosphate (e.g. Page 5-4 MAN 0384, 67 Viewing the results Chapter 5 Removing a record from the Records tab There are two ways to remove a record from the Records tab: Using the Show Fields dialogue, select the field to remove from the righthand list, then press the Remove button. the new changes must be saved (by selecting User-Save). Hydro 2000S/G user manual (English) 09 June 2017 User manual for the Hydro 2000S and Hydro 2000G wet sample dispersion units used with the Mastersizer 2000 instrument Login Email address * Password * Login Forgotten password? When a button is selected an area can be dragged on the report which will then contain the selected item. Try making an SOP measurement using single dairy cream. User manual issue 1.0 for the Mastersizer 2000 and 2000E instruments. Welcome to Bridgit @ CSU The Software Used To Data Conference. Use the pipette to add the sample to the dispersion unit tank. The peak of the frequency curve gives the modal diameter, the most commonly occurring particle diameter. Administrators, users and permissions One or more persons are set up as administrator. Changes to the graph and table format will be reflected in any printouts of the selected report. The data can be displayed in a number of ways which can be altered using the properties box. The Laser Diffraction Particle Sizing (Malvern Mastersizer) uses laser diffraction techniques to measure the size of particles that could be suspensions of solid particles, emulsion droplets, or A measurement file can contain one or more records (see Chapter 7 for details on handling measurement files). 2. ill 1874 Page 9-6 MAN 0384, 113 Advanced features Chapter 9 To transform a result in a manual measurement: 1. Result this tab is displayed when the software is calculating the size distribution. CMA113 MADE IN CHINA 1. The stack has limited support for Bluetooth applications compared to other Windows-based, Quantum 960H DVR range Quick User guide Quick user guide for the Vista Quantum 960H range of DVRs, models included QX960H08-xxx QX960H16-xxx QP960H04-xxx QP960H08-xxx QP960H16-xxx Full manual found on, FlashCut CNC Section 5 Tutorial 259 5. A typical Measurement window is shown below. Changes to the frequently used lists can be made by clicking on the Materials or Dispersants buttons which open up the material/dispersant databases. There are two software modules: The main application, described below. D(v, 0.5) is the size in microns at which 50% of the sample is smaller and 50% is larger. Select the Material tab. 2. Once 21 CFR part 11 security is enabled, it cannot be disabled. A standard template Result Analysis(M) is supplied that exports all fields of the standard report page Result Analysis(M). Manual However, obscuration settings are the preferred method for making dry measurements. Turn, Migrating to Excel 2010 - Excel - Microsoft Office 1 of 1 In This Guide Microsoft Excel 2010 looks very different, so we created this guide to help you minimize the learning curve. Selecting the Default check box will return the limits to the system defaults. To organize and, Soft-Touch TM Bluetooth Laser Mouse 410-XXXXXXXXXXX 1 YEAR LIMITED WARRANTY: We pride ourselves on the quality of our products. Mastersizer 2000 Page 1-5, 20 Chapter 1 Introduction to this manual Malvern website - The Malvern Instruments website offers a comprehensive range of material characterisation resources for use by customers 24 hours a day, seven days a week. i Note If a large number of records are found in the search, it may take some time to display the search results as all measurement files must first be loaded. The problem of the sample settling out within the beaker can be solved by using a pipette to continually stir the sample. Remember that the Mastersizer measurement is fundamentally a measurement of the volume distribution - transforming the result into a surface, length or number distribution is a mathematical process that may amplify any error in the original result, especially at the fine end of the size distribution. The list box on the left shows all fields available that can be added to the records tab. Setting up user groups. A dry measurement cell used on the Scirocco 2000/2000M, detailed in their manuals. The target obscuration values can be set by the user; see Chapter 9. By reducing the result range, the characteristics of the expected result distribution are isolated. It will be clear that there is a size dependence; an obscuration of 30% means a widely varying volume concentration dependent on size. The pressure release or temperature rise reduces the solubility of gases, resulting in bubble formation in the pipes and tank etc. Page 6-12 MAN 0384, 85 Understanding the views Chapter 6 Derived distribution parameters The third point is that the analysed distribution is expressed in a set of size classes which are optimised to match the detector geometry and optical configuration giving the best resolution. Support for hopper fed Scirocco 2000 dry powder feeder added. Mastersizer 2000 Page 5-1, 64 5 Chapter 5 Displaying the information Viewing the results Open a measurement file by selecting File-Open. The result is expressed in terms of equivalent spheres. This list gives commonly used dispersants with their refractive indices: Dispersant Refractive index Water 1.33 Ethanol 1.36 Propan-2-ol (Isopropyl-alcohol) 1.39 Dimethyl Digol 1.41 Butanone 1.38 Hexane 1.38 Acetone 1.36 The Sample Dispersion and Refractive Index guide gives refractive index information for many more dispersants. The sample is measured and the result (size distribution) calculated. Select the Advanced button in the Specify new result calculation section. The Mastersizer 2000E is shown with a Hydro 2000MU. Expressing the Beer-Lambert law in terms of relative transmission and re-arranging to solve for absorbance gives: = Ln T b (1) Volume concentration The term contains information about the concentration and size of the particles. The tube from the dispersion unit to the cell must be connected to the Cell in connector. A table or graph can also be copied by selecting the item then selecting Edit- Copy Table or Edit-Copy Graph. The narrower the distribution, the smaller the span becomes. Depending on the SOP, a dialogue may appear asking the user to document the measurement (add comments and observations). A single search criterion can be altered or deleted by selecting the Edit and Delete buttons in the Find Measurements dialogue. Essentials Manual This manual covers: Site requirements all the physical requirements for positioning the system. This is the recommended method of operation and is suited to beginners or when routinely measuring the same type of sample. Malvern Mastersizer 2000 Instructions are also given on how to install the Malvern software if the user upgrades the computer system. Information is also given on basic use of the Hydro 2000G The Measure Background facility automatically makes a measurement of the system containing only clean dispersant when a manual measurement is started, as well as a measurement of the electrical background. Particle size 2000 Integrated systems for particle sizing detailed specification sheets from www.malvern.co.uk/ms2000 Comprehensive particle sizing The Mastersizer 2000 is a practical, reliable solution to the everyday particle sizing needs of industry. These assumptions are incorrect for many materials and for small particles they can give rise to errors approaching 30%, especially when the relative refractive index of the material and medium is close to unity, or when the particles are transparent. Maintenance. A practical use of this is shown in the sieve reports. 2. Mastersizer 2000 Page 1-3, 18 Chapter 1 Introduction to this manual Where to get help Other manuals Several manuals are supplied with the system, each giving information on a different aspect of it. The SOP takes full control of the dispersion unit (unless it s a manual unit), making all adjustments and settings (such as pump speeds and ultrasonic power). Page 5-6 MAN 0384, 69 Viewing the results Chapter 5 The toolbox can be moved anywhere on the screen. The average will be created as a separate new measurement record capable of being saved and recalled. Creating an SOP is very easy. Slurries The act of mixing up a small quantity of concentrated sample, dispersant and additives before it is added to the dispersion unit tank is known as preparing a slurry. For certain materials (most notably certain inks and pigments) the sample has substantially different refractive indices in red and blue light. It is not shown on page 3-3 of the current Essentials manual. The Measurement Display dialogue will appear: 2 1 ill 7753 The status area at the bottom left of the dialogue always says what is going on in the measurement. This is the primary function of a manual measurement. To reduce the result range in an SOP: 1. Page 4-14 MAN 0384, 51 Making measurements - a tutorial Chapter 4 5. 7. This is governed by these search buttons: New search - clears all criteria currently set. To use this website, you must agree to our, Getting Started. The Malvern software is supplied with many standard reports that each display the information in a specific way. When analysing particles suspended in a liquid dispersant, one of the most important decisions is which liquid to use. The residual shown in the Measurement Parameters view indicates how well the calculated data fitted the measurement data. Selecting one of these closes the box. Wild cards can be used to narrow down the search. Select OK to add the search criterion to the list box in the previous dialogue. The dialogue is split into two sides. This allows the measurement to be repeated at a later date. ill 4948 Page 6-2 MAN 0384, 75 Understanding the views Chapter 6 Result-over plot (also known as cumulative oversize ) similar to the result-under plot except that the result is in the form % of sample above a certain size of particle. Check the sample and dispersant to see if they are suitable before a measurement is made. Pressing OK changes the security settings. The particle size distribution v i is the relative volume in size-class i with mean diameter d i. Q i - the mean extinction term for size-class i - is calculated from scattering theory and is a function of the optical properties of the particle and dispersant media. how fast should the stirrer be? Delivering the data you need for outcomes you can trust, The foundation for todays advanced laser diffraction systems, Gold standard protein stability analysis for the regulated environment, Gold standard protein stability analysis for research applications, Fully automated, hands free ITC for increased productivity, The Gold Standard for measuring affinity and stoichiometry, High sensitivity measurement of all binding parameters, Research insights into biomolecular interactions, Rapid, automated, component-specific particle characterization in a single, integrated platform with one-year subscription to Wileys KnowItAll Raman Identification Pro package, Rapid, automated particle size and particle shape analysis, Advanced particle characterization made easy. Select Configure-Existing SOP. Web the mastersizer 3000 is the worlds leading particle size analyzer for accurate and rapid particle size measurements. Specific Surface Area (SSA) the total area of the particles divided by the total weight. I 0 is the intensity of the laser beam measured at the receiver when no sample is present and I is the intensity with sample in the beam. Creating an export template New export templates can be created (or existing ones modified) by selecting Configure-Data export templates to open this dialogue: Selecting New Template adds a new template name in the Available Templates list and then gives the user the option of changing the template s name. Graphs Multiple data graphs can be added to a report. Adding a field to the Records tab There are two ways to add a field to the Records tab: Using the Show Fields dialogue this is accessed by selecting View-Select Fields (or right-clicking on the list header). Selecting any of the field headers will rearrange all records into alpha-numeric order based on that field. The factors may also be individually edited using the factor editor dialogue box, but this should rarely be necessary. Contact the United Kingdom help desk if the local Malvern representative is not available. For example using the button is equivalent to using the File-Open command. However, a record can be re-analysed and the resultant record saved under a new record name. Mastersizer 2000 Page 4-15, 52 Chapter 4 Making measurements - a tutorial Measuring new samples The above procedures are fine if the SOP is set up or all the parameters for a manual measurement specified. Particle size 2000 Integrated systems for particle sizing detailed specification sheets from /ms2000 Comprehensive particle sizing The Mastersizer 2000 is a practical, reliable solution to the everyday, TABLE OF CONTENTS Introduction1 Manual Format2 Log on/off procedures for Windows3 To log on3 To logoff7 Assembly Design Screen8 Part Design Screen9 Pull-down Menus10 Start10, SA-9600 Surface Area Software Manual Version 4.0 Introduction The operation and data Presentation of the SA-9600 Surface Area analyzer is performed using a Microsoft Windows based software package. Page 4-2 MAN 0384, 39 Making measurements - a tutorial Chapter 4 Obscuration range (%) Obscuration graph colour Notes <5 red Add more sample orange Low but usable with a good signal to background ratio green Ideal orange Usable but try to add more dispersant - there s a danger of multiple scattering. D[4,3] is the Volume Weighted Mean or Mass Moment Mean Diameter. Document pressing this button displays a dialogue where the user can document the measurement i.e. Manual Never try to lift the optical bench by this handle. One or more records must be selected before a report can be opened. Stop this button stops the current measurement process. After volume the next most useful distribution type is probably number, which reports the number proportion of particles in each size class.

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